Abbreviations
AcacetylAlaL‐alanineArarylBoctert‐butyloxycarbonylBnbenzylBubutylCANceric ammonium nitratecat.catalyticCMDconcerted metalation–deprotonationDCE1,2‐dichloroethaneDGdirecting templateDIH1,3‐diiodo‐5,5‐dimethylhydantoinDMFN,N‐dimethylformamideDMPU1,3‐dimethyl‐3,4,5,6‐tetrahydro‐2(1H)‐pyrimidinoneequivequivalentEDGelectron‐donating templateEWGelectron‐withdrawing templateGlyglycineHFIPhexafluoroisopropanolKIEkinetic isotope effectLligandLDAlithium diisopropylamidemmetaMemethylMPAAmono‐N‐protected amino acidNMPN‐methylpyrrolidinoneoorthopparaPhphenylPheL‐phenylalaninePinpinacolPivpivaloylPrpropylTBAtetrabutylammoniumTFAtrifluoroacetic acidTBAPF6tetrabutylammonium hexafluorophosphateTFEtrifluoroethanolTHFtetrahydrofuranXPhos2,4′,6′‐diisopropyl‐1,1′‐biphenyl‐2‐yldicyclohexylphosphine
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